2-Bromoethanol → HCID 22631801, compound

HRID 1840431Notes

Reaction equation

[C:1]([S:4][C:5]1[N:6]=[CH:7][N:8]2[CH:12]=[CH:11][S:10][C:9]=12)(=O)[CH3:2].[Br:13]CCO>>[Br:13][CH2:2][CH2:1][S:4][C:5]1[N:6]=[CH:7][N:8]2[CH:12]=[CH:11][S:10][C:9]=12

Participants

Reactant 2

HCID 108982-Bromoethanol

HCID 226316637-Acetylthioimidazo[5,1-b]thiazole

Product 1

HCID 22631801HCID 22631801, compound

Procedure

The procedure of Synthesis Example 11b) was repeated, except that 990 mg of 7-acetylthioimidazo[5,1-b]thiazole and 0.461 ml of 2-bromo ethanol were used as the starting compounds. Thus, 1.06 g of 7-(2-bromoethyl)thioimidazo[5,1-b]thiazole was prepared.

Workup

customThe procedure of Synthesis Example 11b)

Sources & evidence

ORD record: ord-96d1f80dc0d0470b8f24087b160628b3
Source dataset: uspto-grants-2004_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06680313B2

Reaction notes

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