Lithium Hydroxide → HCID 23448270, compound

HRID 1840511Notes

Reaction equation

HRID 1840511 reaction equation
C[O:2][C:3]([CH:5]1[CH2:9][CH2:8][CH2:7][CH:6]1[S:10]([CH2:13][CH2:14][CH2:15][O:16][C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)(=[O:12])=[O:11])=[O:4].[OH-].[Li+]>>[O:16]([CH2:15][CH2:14][CH2:13][S:10]([CH:6]1[CH2:7][CH2:8][CH2:9][CH:5]1[C:3]([OH:4])=[O:2])(=[O:12])=[O:11])[C:17]1[CH:18]=[CH:19][CH:20]=[CH:21][CH:22]=1

Participants

3

Reactant 2

HCID 3939Lithium HydroxideHCID 69881109HCID 69881109, compound

Product 1

HCID 23448270HCID 23448270, compoundYield 85.9%

Procedure

Prepared in the same manner as Example 14 from Example 12 (163 mg) and lithium hydroxide (105 mg) to give the title compound (134 mg) as a white solid.

Sources & evidence

ORD record
ord-1ad1e2c710fb485993e712e928f46202
Source dataset
uspto-grants-2004_01
Patent number
US06680338B2

Reaction notes

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