HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-METHYL-PIPERIDINE HYDROCHLORIDE → HCID 69820426, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-METHYL-PIPERIDINE HYDROCHLORIDE | HCID 521119 | — |
| Reactant | HCID 131724321 | HCID 131724321 | — |
| Product | HCID 69820426 | HCID 69820426 | — |
Reaction Steps
The same procedure as in Example 1.5 is used. Thus, starting with 1,1-dimethylethyl [(S)-4-(5-aminopyrid-2-yl)-1-[(4-methylpiperid-1-yl)carbonyl]butyl]carbamate (10.2 g; 26.0 mmol), 9.5 g of 1-[(2S)-2-amino-5-(5-aminopyrid-2-yl)-1-oxopentyl[-4-methylpiperidine hydrochloride are obtained in the form of a hygroscopic amorphous powder, which is used without further purification in the following step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06680329B2 |
| Source dataset | uspto-grants-2004_01 |
| ORD ID | ord-eb97946480424532ac73c5f453d7e591 |
| Source note | uspto-grants-2004_01 |