HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methoxyindole → 5-Methoxy-3-(piperidin-4-yl)-1H-indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methoxyindole | HCID 13872 | — |
| Reactant | Piperonylamine | HCID 2723901 | — |
| Product | 5-Methoxy-3-(piperidin-4-yl)-1H-indole | HCID 43224 | — |
Reaction Steps
This compound was prepared following the procedure described in Example 1 (parts A and B) starting with 5 g (33.9 mmol) of 5-methoxyindol and 13.2 g (86.2 mmol) of 4-piperidone monohydrate hydrochloride. After the usual work-up 6.5 g (83% of yield) of the desired product were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06683096B2 |
| Source dataset | uspto-grants-2004_01 |
| ORD ID | ord-958a33719ae745398d8dd5da09b83fb1 |
| Source note | uspto-grants-2004_01 |