Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
lithium aluminium hydride THF → [4-(3,4-Dichlorophenyl)-2-pyridinyl]methanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | lithium aluminium hydride THF | HCID 68718528 | — |
| 반응물 | 4-(3,4-Dichloro-phenyl)-pyridine-2-carboxylic acid methyl ester | HCID 69038928 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | [4-(3,4-Dichlorophenyl)-2-pyridinyl]methanol | HCID 23445021 | — |
반응 단계
The title compound, MS: m/e=252.0 ([M−H]−) was obtained as a light brown oil (94% yield) by the reaction of 4-(3,4-dichloro-phenyl)-pyridine-2-carboxylic acid methyl ester with 1M lithium aluminum hydride/THF solution in THF at 20° C. for 1 h followed by chromatographic purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06683097B2 |
| 출처 데이터셋 | uspto-grants-2004_01 |
| ORD ID | ord-b309bc0be4c84e2abb550bfa712706bc |
| 출처 메모 | uspto-grants-2004_01 |