huagongshe.com
HRID1841368

反应详情

EQUATION

反应方程式

HRID 1841368 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)c1cc(C)cc([N+](=O)[O-])c1O
HCID736162

2'-Hydroxy-5'-methyl-3'-nitroacetophenone

C9H9NO4

结构：Cc1cc(C=O)ccc1OCc1ccccc1
HCID20298646

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(C(=O)/C=C/c2ccc(OCc3ccccc3)c(C)c2)c(O)c([N+](=O)[O-])c1
HCID23444716

未命名化合物

收率 66.2%

PROCEDURE

实验过程

2-Hydroxy-5-methyl-3-nitroacetophenone (345 mg, 1.76 mmol) and 3-methyl-4-benzyloxybenzaldehyde (400 mg, 1.76 mmol) were reacted according to the same procedure as Preparation 22 to give 470 mg (Yield 66%) of the title compound.

WORKUP

后处理

  1. customaccording to the same procedure as Preparation 22