HuagongsheHuagongshe Chemistry Print Report · For research reference only
2'-Hydroxy-5'-methyl-3'-nitroacetophenone → (E)3-[4-(benzyloxy)-3-methylphenyl]-1-(2-hydroxy-5-methyl-3-nitrophenyl)-2-propen-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2'-Hydroxy-5'-methyl-3'-nitroacetophenone | HCID 736162 | — |
| Reactant | 4-(Benzyloxy)-3-methylbenzaldehyde | HCID 20298646 | — |
| Product | (E)3-[4-(benzyloxy)-3-methylphenyl]-1-(2-hydroxy-5-methyl-3-nitrophenyl)-2-propen-1-one | HCID 23444716 | 66.2% |
Reaction Steps
2-Hydroxy-5-methyl-3-nitroacetophenone (345 mg, 1.76 mmol) and 3-methyl-4-benzyloxybenzaldehyde (400 mg, 1.76 mmol) were reacted according to the same procedure as Preparation 22 to give 470 mg (Yield 66%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06683095B2 |
| Source dataset | uspto-grants-2004_01 |
| ORD ID | ord-d2ba460c72f7400984b646cdbcde8b49 |
| Source note | uspto-grants-2004_01 |