HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86588089, compound → HCID 69823968, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86588089 | HCID 86588089 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 69823968 | HCID 69823968 | 44.5% |
Reaction Steps
To 1-[(2-methoxyquinoxalin-3-yl)N-methylaminocarbonyl]-4-(3,5-dinitrophenyl)piperazine dissolved in ethanol (30 ml), 10% palladium/carbon (10 mg) was added. The mixture was hydrogenated for 4 hours, and then filtered to remove the 10% palladium/carbon. The filtrate was concentrated and purified by column chromatography to obtain the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06683184B2 |
| Source dataset | uspto-grants-2004_01 |
| ORD ID | ord-ab56bbfeba9e425d9619fed7892240dd |
| Source note | uspto-grants-2004_01 |