HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dibromobutane → [4-(4-Bromo-butoxy)-phenyl]-carbamic acid tert-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dibromobutane | HCID 8056 | — |
| Reactant | N-Boc-4-hydroxyaniline | HCID 2756771 | — |
| Product | [4-(4-Bromo-butoxy)-phenyl]-carbamic acid tert-butyl ester | HCID 68615222 | — |
Reaction Steps
In analogy to example 1.4, reaction of (4-Hydroxy-phenyl)-carbamic acid tert-butyl ester with 1,4-dibromobutane yielded [4-(4-Bromo-butoxy)-phenyl]-carbamic acid tert-butyl ester, MS: 344 (MH+, 1Br).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06683201B2 |
| Source dataset | uspto-grants-2004_01 |
| ORD ID | ord-8c39cbd9c4cb450ba2fc4748696ef333 |
| Source note | uspto-grants-2004_01 |