Diethylamine → HCID 10135895, compound

HRID 1841602Notes

Reaction equation

HRID 1841602 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([O:8][C:9](=[O:24])[N:10]([C:12]2[CH:17]=[CH:16][C:15]([O:18][CH2:19][CH2:20][CH2:21][CH2:22]Br)=[CH:14][CH:13]=2)[CH3:11])=[CH:4][CH:3]=1.[CH2:25]([NH:27][CH2:28][CH3:29])[CH3:26]>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([O:8][C:9](=[O:24])[N:10]([C:12]2[CH:17]=[CH:16][C:15]([O:18][CH2:19][CH2:20][CH2:21][CH2:22][N:27]([CH2:28][CH3:29])[CH2:25][CH3:26])=[CH:14][CH:13]=2)[CH3:11])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 8021DiethylamineHCID 68615035HCID 68615035, compound

Product 1

HCID 10135895HCID 10135895, compound

Procedure

In analogy to example 17.1, reaction of [4-(4-Bromo-butoxy)-phenyl]-methyl-carbamic acid 4-chloro-phenyl ester with diethylamine yielded [4-(4-Diethylamino-butoxy)-phenyl]-methyl-carbamic acid 4-chloro-phenyl ester, MS: 405 (MH+).

Sources & evidence

ORD record
ord-591df04d277e4703a7082917536dcf2d
Source dataset
uspto-grants-2004_01
Patent number
US06683201B2

Reaction notes

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