HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 131732407, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 131732405 | HCID 131732405 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 131732407 | HCID 131732407 | — |
Reaction Steps
Tetraacetyl-(p-(pyridinylhydroxymethyl)phenoxy)-β-galactose (600 mg, 1.1 mmol) is dissolved in 15 ml of CH2Cl2. SOCl2 (143 mg, 88 μl, 1.2 mmol) is added dropwise and the solution is left stirring for 1 hour. The solvent is evaporated under vacuum. The product is obtained pure and quantitatively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08945514B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-ce152e9ac4834ef2a1950f5e2f9b0dd4 |
| Source note | uspto-grants-2015_02 |