Ethylene Glycol → Ethane-1,2-diol--propane-1,2,3-triol (1/1)

HRID 1841846Notes

Reaction equation

HRID 1841846 reaction equation
O.[CH2:2]([OH:5])[CH2:3][OH:4].CCCCC(CC[CH:15]([O:20]S([O-])(=O)=O)CC(C)C)CC.[Na+]>[Cu]=O.[O-2].[Zr+4].[O-2].OCC(CO)O>[CH2:2]([OH:5])[CH2:3][OH:4].[OH:4][CH2:3][CH:2]([CH2:15][OH:20])[OH:5]

Participants

7

Reactant 3

HCID 174Ethylene GlycolHCID 962WaterHCID 23665772Sodium Tetradecyl Sulfate

Product 1

HCID 3084966Ethane-1,2-diol--propane-1,2,3-triol (1/1)

Reagents, catalysts & solvents 3

HCID 14829Copper oxideCatalystHCID 6452892Zirconium oxideCatalystHCID 753GlycerolSolvent

Procedure

A copper oxide dispersion was produced by mixing 2.0 g NanoArc® copper oxide, 5.4 g deionized water, 0.10 g PVP K-30, 0.6 g ethylene glycol, 0.03 g Tergitol® TMN-6, 0.01 g Dynol® 604, and 0.67 g glycerol in a 20 mL vial. 5 g of zirconium oxide milling media was added and the vial was agitated for 60 minutes.

Sources & evidence

ORD record
ord-0d5272bdc5264df0a5151d4677fde73f
Source dataset
uspto-grants-2015_02
Patent number
US08945686B2

Reaction notes

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