HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → HCID 86158515, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | Methyl 16-bromohexadecanoate | HCID 2736822 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86158515 | HCID 86158515 | — |
Reaction Steps
16-bromohexadecanoic acid methyl ester is reacted with sodium azide in acetonitrile for four days at reflux temperature to give the corresponding azide (Zinic et al., Positionally Isomeric Organic Gelators: Structure-Gelation Study, Racemic versus Enantiomeric Gelators, and Solvation Effects, Chem. Eur. J. 2010; 16:3066-82).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08945897B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-9e82479849424fd6ac2d50e6fd3911e4 |
| Source note | uspto-grants-2015_02 |