HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 56941373, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Triethylsilane | HCID 12052 | — |
| Reactant | HCID 66613463 | HCID 66613463 | — |
| Product | HCID 56941373 | HCID 56941373 | — |
Reaction Steps
Trifluoroacetic acid (1 mL) was added to 4-benzyl-N-(3-(pyridin-4-yl)-1-trityl-1H-indazol-5-yl)morpholine-2-carboxamide (0.0217 g, 0.0332 mmol). The reaction was stirred at room temperature for 30 minutes. Triethylsilane (0.1 mL) was added to the reaction and stirred for an additional 5 minutes. The reaction was concentrated in vacuo and purified using prep LC/MS. LC-MS: 414.26 [M+H]. LC/MS RT=1.99 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08946216B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-052b375eecd940049139e0119843f9a5 |
| Source note | uspto-grants-2015_02 |