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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1842047Generated: November 3, 2026

Trifluoroacetic acid → HCID 56941373, compound

https://huagongshe.com/reaction/1842047

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantTriethylsilaneHCID 12052—
ReactantHCID 66613463HCID 66613463—
ProductHCID 56941373HCID 56941373—

Reaction Steps

Trifluoroacetic acid (1 mL) was added to 4-benzyl-N-(3-(pyridin-4-yl)-1-trityl-1H-indazol-5-yl)morpholine-2-carboxamide (0.0217 g, 0.0332 mmol). The reaction was stirred at room temperature for 30 minutes. Triethylsilane (0.1 mL) was added to the reaction and stirred for an additional 5 minutes. The reaction was concentrated in vacuo and purified using prep LC/MS. LC-MS: 414.26 [M+H]. LC/MS RT=1.99 min.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08946216B2
Source datasetuspto-grants-2015_02
ORD IDord-052b375eecd940049139e0119843f9a5
Source noteuspto-grants-2015_02