HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloride methanol → HCID 67469184, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloride methanol | HCID 21893726 | — |
| Reactant | 1,1-Dimethylethyl 3-(2-quinolinyl)-1-azetidinecarboxylate | HCID 58548439 | — |
| Product | HCID 67469184 | HCID 67469184 | 100% |
Reaction Steps
A solution of 3-quinolin-2-yl-azetidine-1-carboxylic acid tert-butyl ester (2.2 g, 7.75 mmol) in 4N HCl/MeOH (20 mL) was stirred at room temperature for 30 min. The reaction mixture was concentrated to give the crude product (1.70 g, 7.75 mmol, yield 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08946230B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-53a987eb0ac1402a81952d1c7079b83e |
| Source note | uspto-grants-2015_02 |