Hydrazine → HCID 178454835, compound

Participants

Reaction Steps

To a solution of benzyl (2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-2-[(dimethylamino)methylene]-5-methyl-3-oxohexanoate (0.13 g, 0.31 mmol) in ethanol (3.1 mL) was added hydrazine (0.28 mL, 3.1 mmol). The mixture was stirred at ambient temperature. After 30 min, the mixture was concentrated to dryness and taken into the next reaction. MS 389.1 (M+1).

Provenance & Evidence