HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 178482267, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 5-fluoro-N-methyl-2-nitroaniline | HCID 22905774 | — |
| Reactant | HCID 178429093 | HCID 178429093 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178482267 | HCID 178482267 | 89% |
Reaction Steps
The reaction and post-treatment were carried out according to Example (16c) using 5-fluoro-N-methyl-2-nitroaniline (US2003-675927, 6.30 g, 37.0 mmol), 6-methylpyridine-2,4-diol (5.09 g, 40.7 mmol), potassium carbonate (5.63 g, 40.7 mmol) and DMF (100 mL) to obtain the title compound (9.06 g, 89%) as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08946264B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-08dc45ac78a04345bec8abf2f99cbcd8 |
| Source note | uspto-grants-2015_02 |