HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitromethane → HCID 66692011, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitromethane | HCID 6375 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-Fluoro-5-methoxybenzaldehyde | HCID 2734872 | — |
| Product | HCID 66692011 | HCID 66692011 | 58.7% |
Reaction Steps
2-Fluoro-5-methoxy-benzaldehyde (4 g, 25.95 mmol) was reacted with nitro methane (1.58 g, 25.95 mmol), 10N NaOH (2.2 mL, 27.24 mmol) to afford 3 g of the product (58.7% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08946260B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-95563d6c339a463f9e109f1393174b1a |
| Source note | uspto-grants-2015_02 |