HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 89963686, compound → HCID 89964245, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 89963686 | HCID 89963686 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 89964245 | HCID 89964245 | 47.4% |
Reaction Steps
6-Methyl-2-(4-methylpyridin-3-yl)-7-nitro-3,4-dihydroisoquinolin-1(2H)-one (I-69f: 940 mg, 3.154 mmol) was reacted with 10% Pd—C (200 mg) and methanol (15 mL) to afford 400 mg of the product (36% yield). LCMS: 79.19%, m/z=268.1 (M+1)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08946260B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-accdc8ab09fc4367909e841624b886d6 |
| Source note | uspto-grants-2015_02 |