Hydrazine hydrate (1:1) → 1H-pyrrole-2-carbohydrazide

Participants

Reaction Conditions

Reaction Steps

Hydrazine monohydrate (31.0 g, 620 mmol) was added to a mixture of methyl 1H-pyrrole-2-carboxylate (10 g, 77.5 mmol) and methanol (100 ml) followed by stirring at 65° C. for 15 h. The mixture was evaporated and the product was isolated as a crystalline solid.

Provenance & Evidence