HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 56952846, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 56952352 | HCID 56952352 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 56952846 | HCID 56952846 | — |
Reaction Steps
To an EtOH (7 mL) solution of N-{6-[2-fluoro-4-(methylamino)phenoxy]pyridin-3-yl}-4-phenoxybenzamide (0.34 g) was added 6 M HCl (0.14 mL) at 0° C. The resultant mixture was stirred at 0° C. The resulting precipitate was recrystallized from EtOH/H2O to give the title compound as a white powder (0.28 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08946437B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-706d98226c6e45aa9525ebc462122593 |
| Source note | uspto-grants-2015_02 |