HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 56952745, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 56952644 | HCID 56952644 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 56952745 | HCID 56952745 | — |
Reaction Steps
To an EtOH (3 mL) solution of N-{6-[2-Methyl-4-(methylamino)phenoxy]pyridin-3-yl}-4-(trifluoromethyl)benzamide (0.30 g) was added 6 M aqueous HCl (0.13 mL) at 0° C. The resultant mixture was stirred at 0° C. The resulting precipitate was recrystallized from EtOH/H2O, giving the title compound as a white powder (0.20 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08946437B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-2b4e9382fb0d4b408599d9a4f955f535 |
| Source note | uspto-grants-2015_02 |