HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 86664521, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 67217646 | HCID 67217646 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86664521 | HCID 86664521 | — |
Reaction Steps
350 mg 3-benzyloxy-5-chloro-4-methyl-benzoic acid in 10 ml acetonitrile are combined with 0.60 ml thionylchloride and gently refluxed for 15 minutes. Then the reaction mixture is evaporated down and evaporated again with toluene. The acid chloride is further reacted without any further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08946438B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-24ee449512e54bac8ab18a0d55756573 |
| Source note | uspto-grants-2015_02 |