HuagongsheHuagongshe Chemistry Print Report · For research reference only
9-Borabicyclo(3.3.1)nonane → HCID 66768828, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 9-Borabicyclo(3.3.1)nonane | HCID 78966 | — |
| Reactant | 1-Boc-4-Methylenepiperidine | HCID 2756808 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 66768828 | HCID 66768828 | — |
Reaction Steps
6.29 ml of a 0.5 M solution of 9-borabicyclo[3.3.1]nonane in tetrahydrofuran are added to 620 mg tert-butyl 4-methylene-piperidine-1-carboxylate under an argon atmosphere, and the reaction mixture is refluxed for 1 h. After cooling to ambient temperature the reaction solution is further reacted without any further working up.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08946438B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-838f659798fa485c96891697bd5bd65c |
| Source note | uspto-grants-2015_02 |