HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58493959, compound → HCID 58493995, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58493959 | HCID 58493959 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 58493995 | HCID 58493995 | — |
Reaction Steps
A mixture of 14.5 g 5-tert-butyl-1-methanesulphonyl-2-methoxy-3-nitro-benzene, 3.0 g 10% palladium on charcoal and 250 ml of methanol is shaken for 6 h at ambient temperature under a hydrogen atmosphere (50 psi). Then the catalyst is filtered off and the filtrate is evaporated to dryness.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08946438B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-7265cae222a148f29e47ddbf713a48a2 |
| Source note | uspto-grants-2015_02 |