Oxalyl chloride → HCID 86719134, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of compound 5c (1.0 g, 2.2 mmol) in CH2Cl2 (10 mL) was added (COCl)2 (0.8 g, 6.6 mmol) dropwise at 0° C. Then this mixture was stirred at 0° C. for 2 h and concentrated to obtain compound 5d (1.0 g, 100%).

Provenance & Evidence