Citric Acid → HCID 86662969, compound

Participants

Reaction Steps

To a solution of 100 mg (0.58 mmol) rasagiline in 1 ml acetone a solution of 117 mg (0.61 mmol, 1.05 eq) anhydrous citric acid in 1 ml warm acetone was added. The solution became turbid during addition forming a waxy precipitate. The supernatant was removed and the wax was washed with 2 ml acetone twice using sonication. On drying in high vacuum a white solid foam was obtained. Drying was continued for 6 h on high vacuum (120 mg, 0.33 mmol, 57%).

Provenance & Evidence