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HRID1845048

反应详情

EQUATION

反应方程式

HRID 1845048 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)c1cccc2[nH]c(N)nc12
HCID24730367

Methyl 2-amino-1H-benzimidazole-4-carboxylate

C9H9N3O2

2 次

结构：COC(=O)c1cc(-c2ccncc2)cc([N+](=O)[O-])c1N
HCID66940533

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)c1cc(-c2ccncc2)cc2[nH]c(N)nc12
HCID66940503

未命名化合物

收率 50%

PROCEDURE

实验过程

0.25 g (50% overall yield) of 2-amino-6-pyridin-4-yl-1H-benzoimidazole-4-carboxylic acid methyl ester was synthesized according to procedures described for the synthesis of 2-Amino-1H-benzoimidazole-4-carboxylic acid methyl ester (intermediate A) starting from 0.5 g (1.8 mmol) of above synthesized 2-Amino-3-nitro-5-pyridin-4-yl-benzoic acid methyl ester. LCMS: 269 (M+1)+.