HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 66940393, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methyl 3-amino-5-fluoro-2-nitrobenzoate | HCID 58724451 | — |
| Reactant | HCID 178519536 | HCID 178519536 | — |
| Product | HCID 66940393 | HCID 66940393 | — |
Reaction Steps
3.0 g (14.0 mmol) of 3-amino-5-fluoro-2-nitro-benzoic acid methyl ester in 1.6 g (15.4 mmol) of triethylamine and 2.1 g (15.4 mmol) of NaOBn/BnOH was heated at 60° C. for 0.5 h to produce 3-amino-5-benzyloxy-2-nitro-benzoic acid benzyl ester. LCMS: 380 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08946259B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-6b9d53ad51614b8991d92ef0e95e1de2 |
| Source note | uspto-grants-2015_02 |