HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane ethanol → HCID 58483478, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane ethanol | HCID 21584144 | — |
| Reactant | HCID 86658671 | HCID 86658671 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 58483478 | HCID 58483478 | — |
Reaction Steps
Prepared analogously to Example 4b from N-(4-bromophenyl)-2-(2,2-difluoroethyl)oxy-5-nitronicotinic acid amide and Ra-Ni in THF. Yield: (quantitative). MS [m+H]+=372 (Br-isotope pattern); TLC: Rf=0.60 (silica gel, DCM:EtOH 9:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08951999B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-9d5769b374b748c99c4a220af8db799f |
| Source note | uspto-grants-2015_02 |