HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 58483437, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 58483415 | HCID 58483415 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 58483437 | HCID 58483437 | — |
Reaction Steps
Prepared analogously to example 45f with 2-fluoro-6-chloro-3-[(2,2,2-trifluoro-1,1-dimethylethyl)carbonylamino]methyl-benzoic acid ethylester (1.02 g; 2.76 mmol) in 1 M aq. NaOH with 25 mL EtOH. The solvent was evaporated, diluted with 4 M aq HCl and extracted with DCM, dried with Na2SO4 and concentrated i.vac to obtain the subtitle compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08951999B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-5af2a31b625d4ec29a0d16d68c5807d8 |
| Source note | uspto-grants-2015_02 |