HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridoxal 5'-phosphate monohydrate → HCID 178482858, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridoxal 5'-phosphate monohydrate | HCID 38882 | — |
| Reactant | HCID 178482875 | HCID 178482875 | — |
| Catalyst | HCID 178506449 | HCID 178506449 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178482858 | HCID 178482858 | — |
Reaction Steps
Prepared analogously to example 4b with 2-dimethylamino-5-nitro-N-(trans-4-trifluoromethylcyclohexyl)-benzamide (50 mg; 0.14 mmol) with Pd/C/H2 (15 mg/50 psi) in 10 mL MeOH. Yield: quantitative; MS: [m+H]+=330; HPLC: Rt=1.14 min (Method MC-1)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08951999B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-f97eba87838a405d9ab553c0f59032e4 |
| Source note | uspto-grants-2015_02 |