HuagongsheHuagongshe Chemistry Print Report · For research reference only
Di-tert-butyl dicarbonate → HCID 89964282, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Di-tert-butyl dicarbonate | HCID 90495 | — |
| Reactant | HCID 89964062 | HCID 89964062 | — |
| Reactant | HCID 89964404 | HCID 89964404 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 89964282 | HCID 89964282 | — |
Reaction Steps
tert-butyl allyl(2-bromopyridin-3-yl)carbamate. To a solution of N-allyl-2-bromopyridin-3-amine (1 eq.) and DCM (0.2 M) is added (Boc)2O (1.5 eq.). The solution is stirred at room temperature until judged complete by TLC. The solution is concentrated in vacuo and purified by column chromatography to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952009B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-af0b2763c8034ad091406bc7813507cb |
| Source note | uspto-grants-2015_02 |