Hydrogen Peroxide → HCID 66978330, compound

HRID 1846419Notes

Reaction equation

HRID 1846419 reaction equation
[CH3:1][N:2]1[C:6]2[C:7]([CH3:20])=[CH:8][C:9](B3OC(C)(C)C(C)(C)O3)=[CH:10][C:5]=2[O:4][C:3]1=[O:21].[OH:22]O>C(O)(=O)C>[OH:22][C:9]1[CH:8]=[C:7]([CH3:20])[C:6]2[N:2]([CH3:1])[C:3](=[O:21])[O:4][C:5]=2[CH:10]=1

Participants

4

Reactant 2

HCID 784Hydrogen PeroxideHCID 66978278HCID 66978278, compound

Product 1

HCID 66978330HCID 66978330, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

0.20 g (0.70 mmol) 3,4-dimethyl-6-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-3H-benzoxazol-2-one were dissolved in 2.0 mL glacial acetic acid and combined with 0.40 mL (4.6 mmol) hydrogen peroxide solution (35% in water) and stirred. The precipitate formed was suction filtered, washed with water and dried i. vac.

Workup

  1. customThe precipitate formed
  2. filtrationfiltered
  3. washwashed with water
  4. customdried i

Sources & evidence

ORD record
ord-8291c14d3cf543238666bd4cac2a1330
Source dataset
uspto-grants-2015_02
Patent number
US08952014B2

Reaction notes

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