Water → HCID 86663892, compound

Participants

Reaction Steps

30 mg (0.70 mmol) sodium hydride (55%, suspension in mineral oil) were added to 0.12 g (0.70 mmol) 6-hydroxy-3,4-dimethyl-3H-benzoxazol-2-one in 5.0 ml DMF and the mixture was stirred for 10 min at RT. Then 0.10 g (0.70 mmol) 4,6-dichloropyrimidine was added and the mixture was stirred for 1 h at RT. Then water and EtOAc were added, the organic phase was separated off, dried on sodium sulphate, filtered and evaporated down.

Provenance & Evidence