Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 4-Amino-m-cresol | HCID 17819 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 23312606 | HCID 23312606 | — |
Reaction Steps
4.66 g (37.5 mmol) 4-amino-3-methylphenol, 5.00 mL glacial acetic acid, 0.500 g (6.09 mmol) sodium acetate and 7.87 mL (83.3 mmol) acetic anhydride were combined and stirred for 1 h at 125° C. After cooling to RT, ice water was added to the reaction mixture. The precipitate formed was suction filtered, washed with water and dried under HV.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08952014B2 |
|---|
| Source dataset | uspto-grants-2015_02 |
|---|
| ORD ID | ord-526dca703d27442e80ec308f8e3c46e7 |
|---|
| Source note | uspto-grants-2015_02 |
|---|
