Water → HCID 86663909, compound

Participants

Reaction Steps

36 mg (0.83 mmol) sodium hydride (55%, suspension in mineral oil) were added to 0 10 g (0.68 mmol) 2-hydroxy-2-methylquinoline in 1.5 mL DMF and the mixture was stirred for 15 min. Then 97 mg (0.63 mmol) 4,6-dichloropyrimidine were added and the mixture was stirred overnight at RT. The reaction mixture was mixed with water and left to stand overnight. The precipitate formed was suction filtered, washed with water and dried i. vac.

Provenance & Evidence