HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → 4-methyl-1H-1,3-benzodiazol-6-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | 3,4-Diamino-5-methylphenol | HCID 19907644 | — |
| Product | 4-methyl-1H-1,3-benzodiazol-6-ol | HCID 66978088 | — |
Reaction Steps
276 mg (2.00 mmol) 3,4-diamino-5-methyl-phenol in 3.00 mL formic acid (98%) were refluxed for 1 h. The reaction mixture was then evaporated down and the residue was dried under HV.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952014B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-26b10771afe947749abe705570d3f11b |
| Source note | uspto-grants-2015_02 |