Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | 4-Methyl-3H-benzooxazol-2-one | HCID 12709336 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 66978224 | HCID 66978224 | — |
Reaction Steps
20.0 g (149.99 mmol) aluminium(III) chloride were combined with 5.0 mL DMF, with cooling. After 15 min stirring, first of all 5.0 g (33.52 mmol) 4-methylbenzo[d]oxazol-2(3H)-one and then 5.0 mL (52.90 mmol) acetanhydride were added and the mixture was stirred for 1 h at 80° C. The cooled reaction mixture was mixed with water. The precipitate formed was suction filtered, washed and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08952014B2 |
|---|
| Source dataset | uspto-grants-2015_02 |
|---|
| ORD ID | ord-94ee784c44584a9488698bc5c5d3780a |
|---|
| Source note | uspto-grants-2015_02 |
|---|
