HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropanecarboxylic acid → 2-cyclopropyl-4-methyl-1H-benzo[d]imidazol-6-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropanecarboxylic acid | HCID 15655 | — |
| Reactant | 3,4-Diamino-5-methylphenol | HCID 19907644 | — |
| Product | 2-cyclopropyl-4-methyl-1H-benzo[d]imidazol-6-ol | HCID 66978175 | — |
Reaction Steps
0.55 g (4.00 mmol) 3,4-diamino-5-methyl-phenol and 1.67 mL (20.00 mmol) cyclopropanecarboxylic acid were stirred for 1 h at 120° C. Then the reaction mixture w evaporated down i.vac. and further reacted as crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952014B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-fc3a6a7467e04958b6408727f4cf4d40 |
| Source note | uspto-grants-2015_02 |