HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropanecarboximidamide hydrochloride → HCID 178516636, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropanecarboximidamide hydrochloride | HCID 2781916 | — |
| Reactant | Dimethylmalonat | HCID 6946994 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Product | HCID 178516636 | HCID 178516636 | — |
Reaction Steps
Under a nitrogen atmosphere 1.50 mL (13.06 mmol) dimethylmalonat, 1.60 g (13.27 mmol) cyclopropanecarboxamidine hydrochloride and 15.0 mL (80.80 mmol) sodium methoxide solution (30%) were refluxed for 1.25 h with stirring. The reaction mixture was slightly acidified and the precipitate formed was suction filtered, washed and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952014B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-d075e8bf99e44000b37766e15f75b103 |
| Source note | uspto-grants-2015_02 |