HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 86663917, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4,6-Dichloropyrimidine | HCID 70943 | — |
| Reactant | 2(3H)-Benzoxazolone, 6-hydroxy- | HCID 157167 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86663917 | HCID 86663917 | — |
Reaction Steps
0.20 g (1.34 mmol) 4,6-dichloropyrimidine, 0.21 g (1.39 mmol) 6-hydroxy-2-benzoxazolinone and 0.20. g (1.45 mmol) potassium carbonate in 2.0 mL DMF were stirred for 2 h at RT. The reaction mixture was mixed with water. The precipitate formed was suction filtered, washed and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952014B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-6ac19a75da584696bc99a4bde18762b6 |
| Source note | uspto-grants-2015_02 |