HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1846479Generated: November 2, 2026
Potassium Carbonate → HCID 86663918, compound
https://huagongshe.com/reaction/1846479
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4,6-Dichloropyrimidine | HCID 70943 | — |
| Reactant | HCID 66978269 | HCID 66978269 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86663918 | HCID 86663918 | — |
Reaction Steps
135 mg (0.62 mmol) (S)-4-methyl-2-(tetrahydrofuran-2-yl)-1H-benzo[d]imidazol-6-ol and 97 mg (0.63 mmol) 4,6-dichloropyrimidine in 2.0 mL DMF were combined with 97 mg (0.70 mmol) potassium carbonate and stirred overnight at 50° C. Then ice water was added and the mixture was extracted with ethyl acetate. The organic phase was concentrated by rotary evaporation i.vac.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08952014B2 |
|---|
| Source dataset | uspto-grants-2015_02 |
|---|
| ORD ID | ord-d1b6d4742ccc441d87206dc3be861d8b |
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| Source note | uspto-grants-2015_02 |
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