Water → HCID 66978308, compound

Participants

Reaction Steps

1.30 g (8.02 mmol) 5-methoxy-2-methyl-1H-benzo[d]imidazole and 0.70 mL (8.56 mmol) sulphuryl chloride in 30.0 mL acetic acid were stirred for 2 h. Another 0.3 mL sulphuryl chloride were added and the mixture was stirred for a further 2 h. The reaction mixture was mixed with water and evaporated down i.vac. The residue was stirred with DIPE and isopropanol, suction filtered and dried.

Provenance & Evidence