HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 86663919, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4,6-Dichloropyrimidine | HCID 70943 | — |
| Reactant | HCID 14365009 | HCID 14365009 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86663919 | HCID 86663919 | — |
Reaction Steps
270 mg (1.81 mmol) 4,6-dichloropyrimidine, 330 mg (1.81 mmol) 4-chloro-5-hydroxy-2-methyl-1H-benzo[d]imidazole and 270 mg (1.95 mmol) potassium carbonate in 1.5 mL DMF were stirred for 2 h at RT. The reaction mixture was mixed with water and the precipitate formed was suction filtered, washed and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952014B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-b550eef10a354aa9ad7a9d11ed0adb89 |
| Source note | uspto-grants-2015_02 |