HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 86663921, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4,6-Dichloropyrimidine | HCID 70943 | — |
| Reactant | 7-hydroxy-5-methyl-2H-benzo[b][1,4]oxazin-3(4H)-one | HCID 66978040 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86663921 | HCID 86663921 | — |
Reaction Steps
0.10 g (0.56 mmol) 7-hydroxy-5-methyl-2H-benzo[b][1.4]oxazin-3(4H)-one and 0.10 g (0.73 mmol) potassium carbonate were placed in 2.0 mL DMF. After 15 min 86 mg (0.56 mmol) 4,6-dichloropyrimidine were added andtmw stirred at RT over the weekend. The reaction mixture was mixed with water, the substance was extracted with ethyl acetate and evaporated down i.vac.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952014B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-bbbb97480858481b8d8c1c11f8176123 |
| Source note | uspto-grants-2015_02 |