HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(2-chloro-4-hydroxy-6-nitrophenyl)acetamid → 4-Amino-3-chloro-5-nitrophenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(2-chloro-4-hydroxy-6-nitrophenyl)acetamid | HCID 66978135 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | 4-Amino-3-chloro-5-nitrophenol | HCID 66978338 | — |
Reaction Steps
1.00 g (4.24 mmol) N-(2-chloro-4-hydroxy-6-nitrophenyl)acetamid were refluxed in 10 mL semiconcentrated hydrochloric acid for 2 h. The reaction mixture was evaporated down i.vac. and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952014B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-992c43b86e70488788b654e6c27fc72b |
| Source note | uspto-grants-2015_02 |