HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 86663925, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4,6-Dichloropyrimidine | HCID 70943 | — |
| Reactant | 2,6-Dihydroxy-4-methylbenzothiazole | HCID 66978290 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86663925 | HCID 86663925 | — |
Reaction Steps
0.30 g (1.66 mmol) 6-hydroxy-4-methylbenzo[d]thiazol-2(3H)-one and 0.25 g (1.68 mmol) 4,6-dichloropyrimidine were placed in 2.0 mL DMF. 0.25 g (1.81 mmol) potassium carbonate were added and the mixture was stirred for 2 h at RT. The reaction mixture was mixed with water and stirred overnight. The precipitate formed was suction filtered, washed and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952014B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-0fcd3a531c454f04a074d42754ddef23 |
| Source note | uspto-grants-2015_02 |