HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1846508Generated: October 31, 2026
Potassium Carbonate → HCID 86663927, compound
https://huagongshe.com/reaction/1846508
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4,6-Dichloropyrimidine | HCID 70943 | — |
| Reactant | HCID 66978274 | HCID 66978274 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86663927 | HCID 86663927 | — |
Reaction Steps
74 mg (0.42 mmol) 2-methoxy-4-methyl-1H-benzo[d]imidazol-6-ol and 68 mg (0.44 mmol) 4,6-dichloropyrimidine were placed in 2.0 mL DMF. 0.12 g (0.88 mmol) potassium carbonate were added and the mixture was stirred for 4 h at 50° C. The reaction mixture was combined with ice water, the substance was extracted with ethyl acetate and evaporated down i.vac.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08952014B2 |
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| Source dataset | uspto-grants-2015_02 |
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| ORD ID | ord-f2bc204380f941459aef11ccbe596556 |
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| Source note | uspto-grants-2015_02 |
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