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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1846508Generated: October 31, 2026

Potassium Carbonate → HCID 86663927, compound

https://huagongshe.com/reaction/1846508

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant4,6-DichloropyrimidineHCID 70943—
ReactantHCID 66978274HCID 66978274—
SolventDimethylformamideHCID 6228—
ProductHCID 86663927HCID 86663927—

Reaction Conditions

Temperature50 °C

Reaction Steps

74 mg (0.42 mmol) 2-methoxy-4-methyl-1H-benzo[d]imidazol-6-ol and 68 mg (0.44 mmol) 4,6-dichloropyrimidine were placed in 2.0 mL DMF. 0.12 g (0.88 mmol) potassium carbonate were added and the mixture was stirred for 4 h at 50° C. The reaction mixture was combined with ice water, the substance was extracted with ethyl acetate and evaporated down i.vac.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08952014B2
Source datasetuspto-grants-2015_02
ORD IDord-f2bc204380f941459aef11ccbe596556
Source noteuspto-grants-2015_02