HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → N-(4-fluoro-2-(trifluoromethyl)phenyl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 4-Fluoro-2-(trifluoromethyl)aniline | HCID 67853 | — |
| Product | N-(4-fluoro-2-(trifluoromethyl)phenyl)acetamide | HCID 10560920 | — |
Reaction Steps
10.0 g (0.56 mol) 4-fluoro-2-trifluoromethyl-phenylamine were stirred overnight at RT in 40 mL acetic anhydride. The reaction mixture was poured onto 300 g ice water. The precipitate formed was suction filtered, washed with 100 mL water and dried i. vac.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952014B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-9e5bc1e16afa450483b0dd94016e1362 |
| Source note | uspto-grants-2015_02 |